Manifold Gukonjesha
Incamake ya Manifold Gukonjesha
Akuma kamashanyarazi gakoreshwa kenshi nkibikoresho byinjira mugukonjesha.Abashakashatsi bashaka ibikoresho bya farumasi bikora cyangwa gutunganya uduce twa HPLC bakunze gukoresha icyuma gikonjesha mugihe cyintambwe yabo ya mbere muri laboratoire.Icyemezo cyo kugura ubu bwoko bwa firime yumye mubisanzwe bishingiye kubipimo birimo, ariko ntibigarukira gusa:
1. -Umubare wabakoresha muri laboratoire ni mwinshi kandi ibicuruzwa bakora ni bito
2. -Imibare minini yicyitegererezo gito
3. Ingengo yimishinga ntoya
4. Ubwoko bwa banki yubwoko bwibikoresho
5. Hagarika ibicuruzwa byumye ntabwo bikoreshwa mubucuruzi muriki cyiciro
6. Ubushakashatsi bwambere cyane
7. Gutunganya ibicuruzwa byibuze birakenewe
Nubwo umubare munini wa sisitemu nyinshi zaguzwe kandi zihagije kubikorwa biriho, ni ngombwa kumva ko gukoresha imashini yumye ya firigo ifite imbogamizi zijyanye no gukama.Ubwanyuma uyikoresha ntashobora kugenzura uburyo bwo gukonjesha, nkuko babikora mumurongo uhenze kandi utoroshye cyangwa ubwoko bwikonjesha.Ariko, hariho intambwe zishobora guterwa kugirango habeho intsinzi nini kumashanyarazi yumye mugihe ibyo bikoresho byakoreshejwe.Iyi ngingo izasobanura sisitemu yibanze, aho ubushobozi bwabo bugarukira nuburyo bwo kugabanya ibibazo bimwe na bimwe bishobora kubaho mugihe cyo gukonjesha.
Gusobanukirwa Ibice bya Manifold Gukonjesha
Kimwe na firime zose zikonjesha icyuma gikonjesha gifite ibice 4 byibanze.Aba ni:
Sitasiyo yo kongera ibicuruzwa
· Umuyoboro
· Icyuho
Sisitemu yo kugenzura
Sitasiyo Yongeyeho Ibicuruzwa
Sitasiyo yo kongera ibicuruzwa nigice cyibikoresho byinjiza ibicuruzwa kumashanyarazi.Kubijyanye na sisitemu ya sisitemu ibintu byinshi mubikoresho bisanzwe ni flasks.Ibicuruzwa bishyirwa muri flask kandi mubisanzwe bikonjeshwa muburyo bwo kwiyuhagira ubushyuhe buke cyangwa firigo.Tuzaganira kumahitamo yo gukonjesha mubwimbitse nyuma yiyi nyandiko yubuhanga.
Umuyoboro
Kondenseri hafi ya zose zigezweho zikonjesha ni ubuso bukonjesha bukora kugirango uhindure sublimation mugukora a
agace k'umuvuduko muke.Kondenseri ikora kandi kugirango ifate ubushuhe / ibishishwa bityo bikababuza kujya mumashanyarazi.Ibyuma byumye byinshi bitangwa muri "stade imwe"
.Ubushyuhe ntarengwa buri hagati ya - 48C (kuri stade imwe) kugeza kuri 85C (sisitemu ebyiri) ntibisanzwe.Sisitemu zimwe zivanze zirashobora kugera no mubushyuhe buke, nka -105C.Ni ngombwa kumva ko umuvuduko wumuyaga hejuru yurubura atari umurongo ugororotse.Nkuko ubushyuhe bugenda bugabanuka no kugabanya amategeko yo kugabanya kugaruka birakurikizwa.
Sisitemu Vacuum na Pompo ya Vacuum
Umuvuduko wumuyaga hejuru yurubura kuri -48C uhwanye na 37.8 mT.Kuri -85C ni 0,15 mT isobanura itandukaniro rya 37.65
mT.Urashobora kubona ariko ko munsi -85C ubushyuhe bwo hasi butera gusa kugabanuka gake cyane kugabanuka kumuvuduko - muri kimwe cya cumi na ijana bya milliTorr.Mubyukuri, imyuka myinshi yumuyaga hejuru yimeza yasohotse ihagarara hafi -80C kuko kubushyuhe buke itandukaniro ryumuvuduko riba rito.
Pompo ya vacuum kubintu byinshi byumye bikonjesha ni ibyiciro bibiri bizunguruka amavuta ya pompe ya vacuum.Vacuum pompe igamije gusa mugihe kinini cyo gukonjesha gukonjesha ni ugukuraho imyuka idahwitse (azote, ogisijeni, dioxyde de carbone et al) mukumisha.Mugukuraho imyuka idahwitse muri sisitemu pompe vacuum ifasha cyane cyane kurema ibidukikije bya sublimation (ice to vapor itanyuze mucyiciro cyamazi)
Kuri.Kuberako ibyuma byose byuma bikonjesha bifite ibimeneka (kumeneka neza - gusohora ibyuma bitagira umwanda (yego birashobora gusohoka), gasketi, acrylics nibindi hamwe na pinhole nyayo yamenetse muburyo butandukanye hamwe na sisitemu, nko kuri vacuum umuyoboro uhuza hagati kondenseri na pompe ya vacuum) pompe ya vacuum ikora ubudahwema mugihe cyumye cyumye.Mubyukuri NIBA icyuma gikonjesha cyari cyuzuye kandi cyuzuye rwose, iyo pompe ya vacuum imaze gukora hasi yambere irashobora kuzimya kandi ntigikoreshwa ukundi kugeza irangiye.Mubuzima busanzwe ibi ntibishoboka.
Sisitemu yo kugenzura
Igenzura rya sisitemu yo gukonjesha igenda irushaho kuba ingirakamaro mugutandukanya icyuma gikonjesha ikindi.Ingano yo gukoresha no gukoresha inshuti birashobora gutandukana cyane kumashini imwe kurindi.Hatitawe ku kirango, birasabwa ko byikora kuri no guhita byikora biri mubushobozi bwumugenzuzi.Muri laboratoire aho ibyuma byumye bikoreshwa cyane, gukonjesha gukonjesha nuburyo bwo kurangiza kandi nubundi buryo murutonde rurerure rwibikorwa abantu bagomba gukoresha kugirango bagere ku ntego zabo.Ntabwo buriwese ari umuhanga wumye.Kugira imikorere yikora kuri no kuzimya bifasha kwemeza ko uburyo bwiza bwo gutangira no gufunga bikoreshwa mugutanga sisitemu yo kurinda no kuramba.
Igihe cyo kohereza: Mutarama-21-2022